IISc-DST/SAIF NMR Spectrometers (External users)
Submission of samples: Send the samples in an envelope (preferably in a cloth-lined) or cardboard box. The package should be addressed to "The Convener, SIF, IISc NMR Facility, Indian Institute of Science, Bangalore - 560012".
For solution-state NMR: Provide about 5 mg sample for proton NMR and 25 mg for other nuclei, preferably in a small vial. Do not dissolve your sample. We provide the solvent. Please mention if the samples are paramagnetic.
For solid-state NMR: Provide about 300 mg of sample as fine powder. Also make sure that your sample is non-magnetic. Solid-state 1H NMR facility is not available.
Request form:
Fill-in the details in the form and send it along with the samples. The charges are subsidised for academic and government / R&D users; hence the form should carry either an official seal or an accompanying request on an official letterhead.
Results are sent by email within a week of receiving the samples.
Rates for 1D analysis on 400 MHz and 500 MHz solution state NMR spectrometer
S. No | Nuclei | Rate per sample (Rs.) | ||
---|---|---|---|---|
Academic | Government and R&D |
Industry | ||
1 | 1H, 19F (128 scans) | 300 | 900 | 1,500 |
2 | 13C (1028 scans) | 600 | 1,800 | 3,000 |
3 | 1H & 13C (128 scans for 1H and 1028 scans for 13C) | 900 | 2,700 | 4,500 |
Rates for 1D analysis on 600 MHz solution state NMR spectrometer
S. No | Nuclei | Rate per sample (Rs.) | ||
---|---|---|---|---|
Academic | Government and R&D |
Industry | ||
1 | 1H, 19F (128 scans) | 500 | 1,350 | 2,250 |
2 | 13C (1028 scans) | 1,000 | 2,700 | 4,500 |
3 | 1H & 13C (128 scans for 1H and 1028 scans for 13C) | 1,500 | 4,050 | 6,750 |
S. No | Nuclei | Rate per sample (Rs.) | ||
---|---|---|---|---|
Academic | Government and R&D |
Industry | ||
1 | 27Al, 31P & 11B (30 Minutes) | 900 | 2,700 | 4,500 |
2 | 13C (1 Hour) | 1,800 | 5,400 | 9,000 |
3 | 29Si (2 Hour) | 3,600 | 10,800 | 18,000 |
There will be additional charges for advanced experiments and additional scans, as per requirements.
For 1D NMR of other nuclei and other advanced experiments, contact the Facility Manager Dr. Sunita R (sunitar@iisc.ac.in)