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IISc-DST/SAIF NMR Spectrometers (External users)

Submission of samples: Send the samples in an envelope (preferably in a cloth-lined) or cardboard box. The package should be addressed to "The Convener, SIF, IISc NMR Facility, Indian Institute of Science, Bangalore - 560012".

For solution-state NMR: Provide about 5 mg sample for proton NMR and 25 mg for other nuclei, preferably in a small vial. Do not dissolve your sample. We provide the solvent. Please mention if the samples are paramagnetic.

For solid-state NMR: Provide about 300 mg of sample as fine powder. Also make sure that your sample is non-magnetic. Solid-state 1H NMR facility is not available.

Request form:

Solution state

Solid state

Fill-in the details in the form and send it along with the samples. The charges are subsidised for academic and government / R&D users; hence the form should carry either an official seal or an accompanying request on an official letterhead.

Results are sent by email within a week of receiving the samples.

Rates for 1D analysis on 400 MHz and 500 MHz solution state NMR spectrometer

S. No Nuclei Rate per sample (Rs.)
Academic Government and
R&D
Industry
1 1H, 19F (128 scans)   300   900 1,500
2 13C (1028 scans)   600 1,800 3,000
3 1H & 13C (128 scans for 1H and 1028 scans for 13C)   900 2,700 4,500
The tables show the base cost, including GST. Additional cost for deuterated solvents for solution state NMR applies as mentioned below. Chloroform-d and D2O Rs. 100 per sample DMSO-d6 Rs. 300 per sample.

Rates for 1D analysis on 600 MHz solution state NMR spectrometer

S. No Nuclei Rate per sample (Rs.)
Academic Government and
R&D
Industry
1 1H, 19F (128 scans)   500 1,350 2,250
2 13C (1028 scans) 1,000 2,700 4,500
3 1H & 13C (128 scans for 1H and 1028 scans for 13C) 1,500 4,050 6,750
The tables show the base cost, including GST. Additional cost for deuterated solvents for solution state NMR applies as mentioned below. Chloroform-d and D2O Rs. 100 per sample DMSO-d6 Rs. 300 per sample.

Rates for solid state NMR analysis
S. No Nuclei Rate per sample (Rs.)
Academic Government and
R&D
Industry
1 27Al, 31P & 11B (30 Minutes)   900  2,700  4,500
2 13C (1 Hour)  1,800  5,400  9,000
3 29Si (2 Hour)  3,600 10,800 18,000

There will be additional charges for advanced experiments and additional scans, as per requirements.
For 1D NMR of other nuclei and other advanced experiments, contact the Facility Manager Dr. Sunita R (sunitar@iisc.ac.in)